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[1]杨靖,黎莉*,戴立珍,等.白玉兰种子挥发油成分的GCMS分析[J].武汉工程大学学报,2010,(03):47-48.
　YANG Jing,LI Li,DAI Li zhen,et al.Study on constituents of volatile oils from the seeds of Magnolia denudate Desr[J].Journal of Wuhan Institute of Technology,2010,(03):47-48.
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白玉兰种子挥发油成分的GCMS分析(/HTML)
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2010年03期
页码:
47-48
栏目:
化学与化学工程
出版日期:
2010-03-31

文章信息/Info

Title:
Study on constituents of volatile oils from the seeds of
Magnolia denudate Desr
文章编号:
16742869(2010)03004702
作者:
杨靖; 黎莉*; 戴立珍; 黄齐茂; 胡学雷
武汉工程大学化工与制药学院，绿色化工过程教育部重点实验室, 湖北 武汉 430074
Author(s):
YANG Jing;  LI Li;  DAI Lizhen;  HUANG Qimao;  HU Xuelei
School of Chemical Engineering & Pharmacy, Wuhan Institute of Technology; Key Laboratory
for Green Chemical Process of Ministry of Education, Wuhan 430074, China
关键词:
白玉兰; 挥发油; 水蒸气蒸馏; 气质联用
Keywords:
Magnolia denudate Desr;  volatile oil;  steam distillation;  GCMS
分类号:
R284.1
DOI:
-
文献标志码:
A
摘要:
研究了白玉兰种子的挥发油成分.以水蒸汽蒸馏法提取白玉兰种子挥发性成分,用气质联用技术分离测定，结合计算机检索技术对化合物进行结构鉴定，并用色谱峰面积归一化法计算各成分的相对质量分数.结果表明：白玉兰种子挥发油的成分大多为烯类，间伞花烃含量为34.68%，对伞花烃含量为55.16%，β丁香烯的含量为9.26%.初步明确了白玉兰种子挥发油的主要成分及含量，为进一步有效地开发利用该植物提供了一定的科学依据.
Abstract:
The chemical constituents of volatile oil from the seeds of Magnolia denudate Desr. were studied.The volatile components were extracted by steam distillation, and were separated and identified by GC/MS. The components were matched with NIST（National Institute of Standards and Technology）library and the relative contents in percentage were calculated by peak area normalization method in chromatogram.The major components were Benzene,1methyl4(1methylethyl)(34.68%),Benzene,1methyl3(1methylethyl)(55.16%), βcaryophyllene(9.26%).The major components of the seeds of Magnolia denudate Desr. were known and a scientific basis was provided for further development and utilization of the plant through analysis.

参考文献/References:

［1］邱天道.本草外用指南［M］.北京:军事医学科学出版社, 2001：79.
［2］Wang Hong Wu, Lu Xian Ge, Peng Yan Xia. Analysis of the essential oils from the flowers and leaves of Magnolia denudata Desr. in different seasons by gas chromatographymass spectrometry ［J］. Jingxi Huagong, 2007, 24(3):257260.
［3］Fujita S, Ishimatsu Y, Fujita Y.Miscellaneous contributions to the essential oils of the plants from various territories.XLII.On the components of the essential oils of Magnolia denudata Desr ［J］.Yakugaku Zasshi, 1977, 97(11):12161218.
［4］张坚,孙培龙,徐双阳,等.白玉兰精油的化学成分［J］.精细化工,2006,23(4):372374.
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［7］朱雄伟,杨晋凯,胡道伟.辛夷成分及其药理研究综述［J］.海峡药学,2002,14(5):57.
［8］邱琴,刘廷礼,崔兆杰,等.GCMS法测定辛夷挥发油成分［J］.中药材,2001,24(4):269270.
［9］程朝晖,龚春晖,金波,等.辛夷超临界萃取物的气相色谱质谱分析［J］.中国食品添加剂,2003(2):109lll.

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备注/Memo

备注/Memo:
收稿日期：20091213作者简介：杨靖（1984），男，湖北宜昌人，硕士研究生.研究方向：中药活性成分及制剂.指导老师：黎莉，女，教授，硕士研究生导师.研究方向：中药活性成分及制剂.*通信联系人
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