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[1]张细华,颜流水*,汤麦莲,等.气相色谱法测定水中四种菊酯类农药的残留量[J].武汉工程大学学报,2011,(11):35-37.
　ZHANG Xi hua,YAN Liu shui,TANG Mai lian,et al.Determination of four pyrethroid in water by gas chromatography[J].Journal of Wuhan Institute of Technology,2011,(11):35-37.
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《武汉工程大学学报》[ISSN:1674-2869/CN:42-1779/TQ]

卷:
期数:
2011年11期
页码:
35-37
栏目:
化学与化学工程
出版日期:
2011-11-30

文章信息/Info

Title:
Determination of  four pyrethroid in water by gas chromatography
文章编号:
16742869(2011)11003503
作者:
张细华; 颜流水*; 汤麦莲; 罗方舟; 马文强
南昌航空大学环境与化学工程学院，江西 南昌 300063
Author(s):
ZHANG Xihua; YAN Liushui; TANG Mailian; LUO Fangzhou; MA Wenqiang
College of EnvironmentaL and ChemicaL Engineering, Nanchang Hangkong University,Nanchang 330063,China
关键词:
气相色谱; 拟虫类菊酯农药; 生活饮用水; 残留量
Keywords:
gas chromatography; pesticide permethrin; drinking water; residues
分类号:
X131.2
DOI:
-
文献标志码:
AAdoi:10.3969/j.issn.16742869.2011.11.009
摘要:
建立了一种生活饮用水与水源水中菊酯类农药残留量的气相色谱检测方法.以石油醚为萃取剂，利用PE5毛细管色谱柱分离，用GCECD测定联苯菊酯、甲氰菊酯、氯氰菊酯、溴菊酯四种拟虫类菊酯农药的残留量.方法的线性范围0.08~0.4 μg·mL-1,相对标准偏差为3.7%~9.5%，加标回收率为80.2%~108.5%.方法准确、灵敏、可靠，且有机溶剂用量小,验证了方法的实用性.
Abstract:
A gas chromatography method for determinating drinking water and source water pyrethroid pesticide residues was established.Petroleum ether as extraction solvent and capillary column of four pesticide permethrin residues was determined.The linear range of 0.08-0.40 μg.mL-1.The relative standard deviation was 3.7%-9.5%,the recove chromatography,gas chromatography with ECD fenpropathrin,deltamethrin,cypermethrin,bifenthrinry rate was 80.2%-108.5%.The method was accurate,sensitive,reliable,and adaptable.Experiment showed that the approach was practical.

参考文献/References:

［1］马志梅.气相色谱法同时测定生活饮用水中五种菊酯类农药残留量［J］.福建分析测试，2007,16(3）:6164.
［2］农业部农药检定.NY/T7882004农药残留量试验准则(农业部行业标准）［S］.北京:中国标准出版社，2004.
［3］余磊，刘斌.气相色谱法测定大白菜中甲氰菊酯和溴氰菊酯的残留分析［J］.贵州农业科学，2010,38(6）:213215.
［4］徐范，武铁军.甲氰菊酯的气相色谱分析［J］.农药，1996,35(11):1819.

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